Specimen Preparation

Model 681 High Resolution Ion Beam Coater

High Resolution Ion Beam Coating System for SEM and TEM

A unique ion beam based sputter coating system producing continuous, ultra thin, amorphous coatings free of thermal artifacts making them ideal for FESEM and TEM applications. This is an important advantage over traditional coating techniques such as thermal evaporation, magnetron or RF sputtering that produces coarse deposition structures.

Two Compact Ion Sources produce high sputtering rates. Coating times vary from about 10 seconds to 2 minutes depending on target material, ion beam energy and coating thickness.

A Whisperlok™ mechanism provides true "Fast Specimen Exchange"
(<1 minute) thus eliminating venting the complete chamber to atmosphere when loading and unloading samples. A second key feature is providing variable speed sample rotation along with simultaneous rocking to ensure uniform sample coating.
TEM Whisperlok™ Adapters (Optional) offers the ability to accept all makes of side-entry TEM or SEM sample holders. Samples may be coated at low temperatures using TEM cryoholders if required.

Multiple Targets: The target exchange mechanisms permits selection of one of two available target materials within seconds without breaking vacuum. Adding a second target exchange mechanism (Optional) allows the user two additional targets for a total of four target materials. Dormant targets within the chamber are fully shielded from sputter contamination.

The Gatan ion beam coater offers convenience, efficiency and dependability in a compact, bench-top instrument. It produces ultra-fine grained/amorphous and artifact free coatings for the more demanding high-resolution field-emission microscopes. Specimens are coated quickly with negligible specimen heating.

An optional Film-Thickness Monitor (FTM) measures deposition rate continuously and permits improved control of the film thickness.

Specifications

Ion Source  
Ion Guns Two Penning ion guns with miniature rare earth magnets
Ion Beam Energy 1.0keV to 10.0keV
Beam Diameter About 1mm FWHM
Ion Current Density 10mA/cm2 Peak
Gas throughput Argon at 0.1cc/minute/gun
Airlock Assembly  
Sample Holder Accepts 1¼ inch (31mm) Metallographic mounts and multiple SEM stubs
Sample Rotation Variable speed 10-60rpm
Sample Tilt Fixed angle or variable rocking angle (0° - 90°)
Sample Rocking Variable speed 5°/Sec - 36°/sec
Option TEM adapters for side-entry TEM or SEM holders
Coating  
Coating Rate Approximately 0.5 Å/sec for Carbon and 1.5 Å /sec for Chromium at 10.0keV
Coating Area Uniform over a 1 inch diameter
Target Holder One dual target set, externally selectable while under vacuum
Target Materials Choice of four target materials (see complete list)
Vacuum  
Dry Pumping System Two stage diaphragm pump backing a 60l/sec molecular drag pump
Vacuum Gauge Cold-cathode gauge for specimen chamber. Solid state sensor for backing pressure
Specimen Exchange Gatan Patented Whisperlok™, specimen exchange time <1 minute
Liquid-nitrogen Trap Approximately 5 hour capacity (Standard)
Dimension and Utilities  
Overall Size 560mmW x 480mmD x 430mmH (22"W x 19"D x 17"H)
Shipping Weight 45kg (100lbs)
Power Requirements Universal voltage 100VAC - 240VAC, 50/60Hz
User to specify voltage to insure correct line cord
Power Consumption 200 Watts during operation, 100Watts with ion guns off
Gas Requirements Argon gas at 70psi (4.82 bar)
Warranty One year